TY - JOUR
T1 - Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device
AU - Katsikis, Sotirios
AU - Marin-Montesinos, Ildefonso
AU - Pons, Miquel
AU - Ludwig, Christian
AU - Günther, Ulrich L.
N1 - Publisher Copyright:
© 2015, Springer-Verlag Wien.
Copyright:
Copyright 2015 Elsevier B.V., All rights reserved.
PY - 2015/7/26
Y1 - 2015/7/26
N2 - Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.
AB - Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system.
UR - http://www.scopus.com/inward/record.url?scp=84932197142&partnerID=8YFLogxK
U2 - 10.1007/s00723-015-0680-5
DO - 10.1007/s00723-015-0680-5
M3 - Journal articles
AN - SCOPUS:84932197142
VL - 46
SP - 723
EP - 729
JO - Applied Magnetic Resonance
JF - Applied Magnetic Resonance
SN - 0937-9347
IS - 7
ER -