Application of 3D-TOCSY-trNOESY for the assignment of bioactive ligands from mixtures

Lars Herfurth; Thomas Weimar; Thomas Peters

doi:10.1002/1521-3773(20000616)39:12<2097::AID-ANIE2097>3.0.CO;2-9

Application of 3D-TOCSY-trNOESY for the assignment of bioactive ligands from mixtures

Lars Herfurth, Thomas Weimar, Thomas Peters^*

^*Korrespondierende/r Autor/-in für diese Arbeit

Institut für Chemie und Metabolomics

16 Zitate (Scopus)

Abstract

With no prior knowledge of the identity of single components, a complete assignment of a bioactive ligand from a mixture of 15 carbohydrate ligands can be accomplished by utilizing NMR spectroscopy. A 3D-TOCSY-(transfer)NOESY experiment delivered essential information for the critical assignment of the glycosidic linkage type of the bioactive disaccharide (see scheme).

Originalsprache	Englisch
Zeitschrift	Angewandte Chemie - International Edition
Jahrgang	39
Ausgabenummer	12
Seiten (von - bis)	2097-2099
Seitenumfang	3
ISSN	1433-7851
DOIs	https://doi.org/10.1002/1521-3773(20000616)39:12<2097::AID-ANIE2097>3.0.CO;2-9
Publikationsstatus	Veröffentlicht - 16.06.2000

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Forschungsschwerpunkt: Infektion und Entzündung - Zentrum für Infektions- und Entzündungsforschung Lübeck (ZIEL)

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10.1002/1521-3773(20000616)39:12<2097::AID-ANIE2097>3.0.CO;2-9

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Application of 3D-TOCSY-trNOESY for the assignment of bioactive ligands from mixtures

Abstract

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